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Product: 109-72-8 N Butyllithium

n-Butyllithium, typ. 15 % solution in Hexane (1.6 M)

C₄H₉Li

CAS Number: 109-72-8
EC Number: 203-698-7
Material REACH Number: 01-2119494906-21-0000

n-Butyllithium, typ. 15 % solution in Hexane (1.6 M) (CAS 109-72-8, molecular formula C4H9Li) is an inorganic chemical supplied as a technical-grade material. It is typically a yellow liquid.

Initiator for olefin polymerization. Alkylating and metalating agent.

Typical specifications include: active base 14.8 - 15.3 % (1.6 M); free base max. 0.3 %; activity min. 98 %.

Under exclusion of air and humidity the solution is fairly stable (decomposition rate at 20 °C: abt. 0.06 %; at 35 °C: abt.

Physical and Chemical Properties
Property Value
IUPAC Name
 
Molecular Weight
64.06g/mol
Appearance
Liquid
Color
Yellow
Flash Point
-35 °C 1,013 hPa (Hexane)
Boiling Point
65 - 70 °C at 1,013 hPa Method: ISO 3405 (Hexane)
Density
ca. 0.68 g/cm3 at 20 °C
Solubility in Water
(Not applicable)

Applications

Initiator for olefin polymerization. Alkylating and metalating agent.

Specifications

Chemical analysis:
  • active base 14.8 - 15.3 % (1.6 M)
  • free base max. 0.3 %
  • activity min. 98 %
  • Cl (covalent) max. 0.03 %
  • mainly LiOC4H9

Handling and Storage

Handling Instructions

Under exclusion of air and humidity the solution is fairly stable (decomposition rate at 20 °C: abt. 0.06 %; at 35 °C: abt. 0.5 % of active material per month). Decomposition does not cause pressure build up in containers. Butyllithium should always be handled under inert gas like nitrogen although hydrocarbon solutions of n-butyllithium in concentrations of LiR up to about 25 % normally do not ignite spontaneously when coming in contact with air. Increase in concentration due to evaporation of solvent results in rising danger of selfignition.

Storage Instructions

After longer storage, solution of Butyllithium tend to form finely dispersed LiH which is very likely to ignite when in contact with air. Pay attention to official safety regulations (see also "Transport regulations" and "GHS Hazard Pictograms", especially fire fighting). Please ask for our Butyllithium brochure.