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Lithium Amide, milled

Lithium Amide, milled

LiNH2

CAS Number:  7782-89-0 EC Number:  231-968-4 REACH Number:  01-2120757139-47-0000

Lithium Amide, milled (CAS 7782-89-0) is an inorganic compound with molecular formula LiNH2. It is supplied as a milled solid.

Lithium Amide is commonly used as a strong base in organic chemical synthesis. Examples include aldol and claisen condensations, deprotonation of amines and elimination reactions.

Lithium Amide reacts readily with moisture and air and should be handled under dry, inert conditions. Consult the SDS and site-specific procedures for compatible materials, fire response, and storage.

Physical and Chemical Properties
Property Value
IUPAC Name
Lithium Amide
Molecular Weight
22.96g/mol
Appearance
Solid
Color
White To Gray
Boiling Point
(Decomposes below the boiling point.)
Density
1.17 g/cm3 at 20 °C
Bulk Density
ca. 600 kg/m3
Solubility in Water
(Not applicable)
Additional Properties
Particle size: typ. 90 % < 0.4 mm

Applications

Claisen condensation, Aldol condensation. Alkylation of nitriles, ketones, amines, alkynes. Synthesis of ethynyl compounds and antihistamines. Transesterification. Catalyst for the anionic polymerization of acrylonitrile and methacrylonitrile.

Specifications

  • LiNH2 min. 94 %
  • LiH on request

    Method of Analysis

    Determination by acidimetric titration. Detailed description on request.

    Handling Instructions

    Lithium Amide should be handled under inert gas atmosphere. Avoid contact with eyes, skin and clothes as well as inhalation. Dust may form explosive mixture in Air. Lithium Amide decomposes in contact with humidity. Pay also attention to the Safety Data Sheet - Section 7.

    Storage Instructions

    Lithium Amide should be stored in tightly closed containers under exclusion of humidity at gentle temperatures. Keep away from heat, sparks and fire. When stored according to SDS and under exclusion of air and humidity, the material is fairly stable. We still recommend to retest the material 6 months after date of analysis if included on CoA. If not included, use the date of manufacturing for the calculation. Pay also attention to the Safety Data Sheet.

    Legal Disclaimer

    The information presented herein is believed to be accurate and reliable but is presented without guarantee or responsibility on the part of Albemarle Corporation and its subsidiaries and affiliates. It is the responsibility of the user to comply with all applicable laws and regulations and to provide for a safe workplace. The user should consider any health or safety hazards or information contained herein only as a guide and should take those precautions which are necessary or prudent to instruct employees and to develop work practice procedures in order to promote a safe work environment. Further, nothing contained herein shall be taken as an inducement or recommendation to manufacture or use any of the herein materials or processes in violation of existing or future patent.